Capillary Electrophoresis Workshop - Day 2
Time
Topic
Instructor(s)
8:30 – 9:00 a.m. Review Previous Day – Q & A Northrop, McDermot, Jagmin, Heegel
9:00 – 10:00 a.m.

HI Methods – Reaction Mechanisms & Stiochiometry

  1. HI/Red P
  2. Hypophosphorous Acid
  3. Phosphorous Acid
  4. Other
 Northrop
10:00 – 10:15 a.m. Break  
10:15 a.m.– 12:00 p.m.

HI Methods of Manufacturing w/CE and GC/MS Analysis

  1. HI Methods of Manufacture
  2. HI Manufacture – Small Scale
    1. HI/Red P
      1. CE anion analysis
      2. GC/MS analysis
    1. Hypo
      1. CE anion analysis
      2. GC/MS analysis
    1. Phosphorous Acid
      1. CE anion analysis
      2. GC/MS analysis
 Northrop, McDermot, Jagmin, Heegel
12:00 – 1:00 p.m. Lunch  
1:00 – 2:00m p.m.

Completion of morning HI manufacturing

Northrop, McDermot, Jagmin, Heegel
2:00 – 2:15 p.m. Break  
2:15 – 3:00 p.m.

Manufacturing method determination from analytical data

 Northrop
3:00 – 3:15 p.m. Break  
3:15 – 4:30 p.m.

Data Evaluation

  1. Significance of analytical findings
  2. Application of lab data to scene sample evaluation
    		Northrop

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