                                             INSTRUMENT CONTROL PARAMETERS:    Ernie
                                             ---------------------------------------

   C:\MSDCHEM\1\METHODS\THOULI_BENZOS_METHOD1.M
      Fri Aug 02 09:26:28 2024

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  Manual
Mass Spectrometer :  Enabled


 No Sample Prep method has been assigned to this method.

Oven
Equilibration Time                           0.5 min
Max Temperature                              300 degrees C
Slow Fan                                     Disabled
Oven Program                                 On
    40 °C for 0.5 min
    then 30 °C/min to 250 °C for 0.5 min
Run Time                                     8 min




Sample Overlap
Sample overlap is not enabled



Front SS Inlet He
***Excluded from Affecting GC's Readiness State***
Mode                                         Splitless
Heater                                       Off
Pressure                                     Off
Total Flow                                   Off
Septum Purge Flow                            Off
Gas Saver                                    On    20 mL/min After 5 min
Purge Flow to Split Vent                     20 mL/min at 0.5 min


Back SS Inlet He
Mode                                         Split
Heater                                       On    260 °C
Pressure                                     On    7.0699 psi
Total Flow                                   On    25 mL/min
Septum Purge Flow                            On    3 mL/min
Gas Saver                                    On    15 mL/min After 1 min
Split Ratio                                  10 :1
Split Flow                                   20 mL/min


Thermal Aux 2 {MSD Transfer Line}
Heater                                       On
Temperature Program                          On
    250 °C for 0 min
Run Time                                     8 min


Column #1
Restek 13420: 5906.42889
Rxi-5ms Serial # 1649495
350 °C: 15 m x 250 µm x 0.25 µm
In: Back SS Inlet He
Out: Vacuum

(Initial)                                    40 °C
Pressure                                     7.0699 psi
Flow                                         2 mL/min
Average Velocity                             72.524 cm/sec
Holdup Time                                  0.34472 min
Flow Program                                 On
    2 mL/min for 0 min
Run Time                                     8 min





Front Detector FID
***Excluded from Affecting GC's Readiness State***
Heater                                       Off
H2 Flow                                      Off
Air Flow                                     Off
Makeup Flow                                  Off
Const Col + Makeup                           Off
Flame                                        Off
Electrometer                                 On



Back Detector µECD
***Excluded from Affecting GC's Readiness State***
Heater                                       Off
Anode Flow                                   Off
Makeup Flow                                  Off
Const Col + Makeup                           Off
Electrometer                                 On

Aux EPC 4 He
***Excluded from Affecting GC's Readiness State***
Pressure Program                             Off
    10 psi for 0 min
Run Time                                     8 min

Aux EPC 5 He
***Excluded from Affecting GC's Readiness State***
Pressure Program                             Off
    3.88 psi for 0 min
Run Time                                     8 min

Aux EPC 6 He
***Excluded from Affecting GC's Readiness State***
Pressure Program                             Off
    15 psi for 0 min
Run Time                                     8 min


PCM C-1 He
***Excluded from Affecting GC's Readiness State***
Pressure Program                             On
    3.8 psi for 0 min
Run Time                                     8 min


PCM C-2 He
***Excluded from Affecting GC's Readiness State***
Pressure Program                             Off
    1.5 psi for 0 min
Run Time                                     8 min



Signals
 Test Plot                                   Save Off
                                             50 Hz
 Test Plot                                   Save Off
                                             50 Hz
 Test Plot                                   Save Off
                                             50 Hz
 Test Plot                                   Save Off
                                             50 Hz

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 0.00 min

EMV Mode                 : Gain Factor
Gain Factor              : 1.00
Resulting EM Voltage     : 1847

[Scan Parameters]

Low Mass                 : 40.0
High Mass                : 350.0
Threshold                : 150
Sample #                 : 2       A/D Samples    4
Plot 2 low mass          : 50.0
Plot 2 high mass         : 550.0

[MSZones]

MS Source                : 230 C   maximum 250 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US10433616
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      27.107
 IONFOCUS    :      90.157
 ENTRANCE_LE :      25.500
 EMVOLTS     :    1858.824
                               Actual EMV  :    1847.06
                               GAIN FACTOR :       0.97
 AMUGAIN     :     962.000
 AMUOFFSET   :     120.938
 FILAMENT    :       2.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      19.827
 MASSGAIN    :   -1173.000   
 MASSOFFSET  :     -37.000   

                           END OF TUNE PARAMETERS
                      ------------------------------------



                                               END OF INSTRUMENT CONTROL PARAMETERS
                                               ------------------------------------
